DICHLOROETHANOYL CHLORIDE
Dichloroacetyl chloride
CAS: 79-36-7
Molecular Formula: C2HCl3O
DICHLOROETHANOYL CHLORIDE - Names and Identifiers
DICHLOROETHANOYL CHLORIDE - Physico-chemical Properties
| Molecular Formula | C2HCl3O |
| Molar Mass | 147.39 |
| Density | 1.532 g/mL at 25 °C (lit.) |
| Melting Point | <25 °C |
| Boling Point | 107-108 °C (lit.) |
| Flash Point | 66 °C |
| Water Solubility | MAY DECOMPOSE |
| Solubility | Chloroform, Hexanes |
| Vapor Presure | 27mmHg at 25°C |
| Appearance | Liquid |
| Specific Gravity | 1.537 (20/4℃) |
| Color | Clear colorless to light yellow |
| Merck | 14,3053 |
| BRN | 1209426 |
| Storage Condition | 2-8°C |
| Stability | Stable. Combustible. Incompatible with water, alcohols and oxidizing agents. Fumes in air. |
| Sensitive | Moisture Sensitive |
| Refractive Index | n20/D 1.46(lit.) |
| Physical and Chemical Properties | Colorless and irritating liquid. boiling point 108~110 ℃ relative density 1.5315 refractive index 1.4591 solubility is miscible with ether. |
| Use | For organic synthesis and pesticide, pharmaceutical intermediates |
DICHLOROETHANOYL CHLORIDE - Risk and Safety
| Risk Codes | R35 - Causes severe burns R50 - Very Toxic to aquatic organisms |
| Safety Description | S9 - Keep container in a well-ventilated place. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S61 - Avoid release to the environment. Refer to special instructions / safety data sheets. |
| UN IDs | UN 1765 8/PG 2 |
| WGK Germany | 2 |
| RTECS | AO6650000 |
| FLUKA BRAND F CODES | 19-21 |
| TSCA | Yes |
| HS Code | 29159000 |
| Hazard Note | Corrosive/Moisture Sensitive |
| Hazard Class | 8 |
| Packing Group | II |
DICHLOROETHANOYL CHLORIDE - Upstream Downstream Industry
| Raw Materials | Trichloroethylene Trichloroethylene Oxygen |
| Downstream Products | trichloroacetyl chloride Carboprost methylate |
DICHLOROETHANOYL CHLORIDE - Nature
Open Data Verified Data
colorless and irritating liquid. Boiling point 108~110 deg C. The relative density was 1. 5315. Refractive index 4591. Can be miscible with ether, water, ethanol decomposition. Smoke in the air.
Last Update：2024-01-02 23:10:35
DICHLOROETHANOYL CHLORIDE - Preparation Method
Open Data Verified Data
- trichloroethylene and azobisisobutyronitrile (catalyst) were heated to 100 ℃, and oxygen was introduced. The reaction was carried out under a pressure of 6MPA, the temperature of the oil bath was maintained at 110 ° C., the reaction was carried out for 10 hours, and the product dichloroacetyl chloride was distilled off under normal pressure.
- the reaction of the by-product trichloroethylene oxide with amine compounds such as methylamine, triethylamine and pyridine may also be converted into dichloroacetyl chloride.
Last Update：2022-01-01 10:32:16
DICHLOROETHANOYL CHLORIDE - Use
Open Data Verified Data
for the synthesis of vinyl insecticides, also used in wool felting finishing, bleaching, decolorization, preservation, sterilization, Disinfection.
Last Update：2022-01-01 10:32:15
DICHLOROETHANOYL CHLORIDE - Safety
Open Data Verified Data
- This product is highly irritating. Rat oral LD50 2.46g/kg. The production workshop should be ventilated and the production equipment should be closed. The operator shall wear protective equipment and pay attention to the protection of eyes and skin.
- tightly sealed in brown glass bottles, external use of wooden box protection, sun protection, moisture, storage in a cool, dry, ventilated place. It shall be stored and transported according to the regulations for irritant substances.
Last Update：2022-01-01 10:32:16
DICHLOROETHANOYL CHLORIDE - Reference Information
| NIST chemical information | information provided by: webbook.nist.gov (external link) |
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | dichloroacetyl chloride is an agent with antitumor and anticancer activity useful in the synthesis of substituted benzothiazoles. used in organic synthesis and pesticides, pharmaceutical intermediates used as intermediates in organic synthesis used in the synthesis of vinyl pesticides, also used in wool felting finishing, bleaching, decolorization, preservation, sterilization, Disinfection, etc. |
| production method | a variety of process routes can be used in the preparation method. The reaction of dichloroacetic acid with chlorosulfonic acid, the reaction of chloroform with carbon monoxide catalyzed by anhydrous aluminum trichloride, the reaction of dichloroacetic acid with phosgene in dimethylformamide, and the oxidation of trichloroethylene can be obtained. Trichloroethylene and azobisisobutyronitrile (catalyst) were heated to 100 ° C., oxygen was introduced, and the reaction was carried out under 0.6MPa pressure. The temperature of the oil bath was maintained at 110 ° C., and the reaction was carried out for 10 hours. The by-product of the reaction, trichloroethylene oxide, can also be converted into dichloroacetyl chloride by reacting with amine compounds such as methylamine, triethylamine and pyridine. |
| category | corrosive article |
| toxicity grade | poisoning |
| Acute toxicity | oral-rat LD50: 2460 mg/kg |
| stimulation data | Skin-moderate in rabbits at 10 mg/24 h; eye-rabbit 50 μg severe |
| flammability hazard characteristics | in case of open flame, high heat, flammable oxidant; Heat or water, acid Decomposition of toxic chloride gas |
| storage and transportation characteristics | The warehouse is ventilated and dried at low temperature; Stored separately from oxidants and acids |
| extinguishing agent | Sand, carbon dioxide |
| toxic substance data | information provided by: pubchem.ncbi.nlm.nih.gov (external link) |
Last Update：2024-04-09 02:00:11
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Raw Materials for DICHLOROETHANOYL CHLORIDE
Downstream Products for DICHLOROETHANOYL CHLORIDE